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Decrystallization/Hydrolysis Vessel

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Decrystallization/Hydrolysis Reaction Vessel
It is just possible to seen the conical, jacketed reactor within the access framework in the photo at right. The skid-mounted, 150 liter vessel is made of 316SS and is coated with a Kynar-like coating for acid resistance. The helical screw mixer is mounted on an orbit arm that sweeps the inner walls of the reactor to insure proper mixing. The direction and speed (e.g., up/down, clockwise/counterclockwise) of the orbit arm and the mixer are adjustable at the vessel's control panel. Feedstock is added through the hinged access port located on the reactor head.

All physical parameters of the batch hydrolysis mixture are monitored. The unit is fully instrumented with several thermoprobes (to measure all fluid temperatures), an IR temperature measurement device (to provide an independent measurement of the surface temperature of the bulk mass), motor amp transducers (to determine bulk turnover rates and to measure kinetic energy inputs due to mixing), and vacuum transducers. The reactor skid features an integral control panel (seen to the right of the vessel) for mixer control and for operation of the condenser unit, mounted above the reactor.

A vacuum pump is used in conjunction with the cooling jacket to cool the mass during the exothermic decrystallization phase. In this mode, the condenser insures that any steam which evolves from the reaction is returned to the vessel for continued mixing.

Upon completion of the reaction, the discharge shoot is opened manually to allow flow into the high viscosity, positive displacement pump and out to either of the plate and frame filter units.

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Copyright © 1998 Arkenol, Inc.    Last modified: January 18, 1999 - MAF